Pesticides
USP <561> List
Method Description
USP <561> pesticide testing using liquid chromatography targets polar and thermally labile pesticides that cannot be analyzed by gas chromatography. This method complements GC analysis to provide comprehensive pesticide screening required by USP standards for pharmaceutical and supplement applications. Many modern pesticides require LC analysis due to their chemical properties and stability characteristics.
Analyte List
| Analyte Name | CAS # | Type |
|---|---|---|
| Acephate | 30560-19-1 | Measured |
| Alachlor | 15972-60-8 | Measured |
| Azinphos-ethyl | 2642-71-9 | Measured |
| Azinphos-methyl | 86-50-0 | Measured |
| Chlorfenvinphos | 470-90-6 | Measured |
| Chlorpyriphos-ethyl | 2921-88-2 | Measured |
| Cypermethrin | 52315-07-8 | Measured |
| Deltamethrin | 52918-63-5 | Measured |
| Diazinon | 333-41-5 | Measured |
| Dichlorvos | 62-73-7 | Measured |
| Dimethoate | 60-51-5 | Measured |
| Ethion | 563-12-2 | Measured |
| Etrimphos | 38260-54-7 | Measured |
| Fenpropathrin | 39515-41-8 | Measured |
| Fensulfothion | 115-90-2 | Measured |
| Fensulfothion Oxon | 6552-21-2 | Measured |
| Fensulfothion Oxonsulfone | 6132-17-8 | Measured |
| Fensulfothion Sulfone | 14255-72-2 | Measured |
| Fenthion | 55-38-9 | Measured |
| Fenthion Oxon | 6552-12-1 | Measured |
| Fenthion Oxon Sulfone | 14086-35-2 | Measured |
| Fenthion Oxon Sulfoxide | 6552-13-2 | Measured |
| Fenthion Sulfone | 3761-42-0 | Measured |
| Fenthion Sulfoxide | 3761-41-9 | Measured |
| Flucythrinate | 70124-77-5 | Measured |
| Fonophos | 944-22-9 | Measured |
| Malaoxon | 1634-78-2 | Measured |
| Malathion | 121-75-5 | Measured |
| Mecarbam | 2595-54-2 | Measured |
| Methamidophos | 10265-92-6 | Measured |
| Methidathion | 950-37-8 | Measured |
| Monocrotophos | 6923-22-4 | Measured |
| Omethoate | 1113-02-6 | Measured |
| Pendimethalin | 40487-42-1 | Measured |
| Permethrin | 52645-53-1 | Measured |
| Phosalone | 2310-17-0 | Measured |
| Phosmet | 732-11-6 | Measured |
| Piperonyl Butoxide | 51-03-6 | Measured |
| Pirimiphos-ethyl | 23505-41-1 | Measured |
| Pirimiphos-methyl | 29232-93-7 | Measured |
| Profenophos | 41198-08-7 | Measured |
| Prothiophos | 34643-46-4 | Measured |
| Pyrethrins Cinerin I | 25402-06-6 | Measured |
| Pyrethrins Cinerin II | 121-20-0 | Measured |
| Pyrethrins Jasmolin I | 4466-14-2 | Measured |
| Pyrethrins Jasmolin II | 1172-63-0 | Measured |
| Pyrethrins Pyrethrin I | 121-21-1 | Measured |
| Pyrethrins Pyrethrin II | 121-29-9 | Measured |
| Quinalphos | 13593-03-8 | Measured |
| lambda-Cyhalothrin | 91465-08-6 | Measured |
| Dimethoate + Omethoate | Total (Sum) | |
| Malathion + Malaoxon | Total (Sum) | |
| Total Fensulfothions | Total (Sum) | |
| Total Fenthions | Total (Sum) | |
| Total Pyrethrins | Total (Sum) |
Technical Data Sheet
Information required by submitted
Please provide an estimated fat content if known. Do not write on the sample or its packaging with solvent-based markers — the ink can contaminate the sample.
Additional information
Modified USP <561> method. The following USP <561> analytes are not covered by the modified method: inorganic bromide (calculated as bromide ion), chlorpyriphos-methyl, dichlofluanid, dithiocarbamates (as CS₂), parathion-methyl/paraoxon-methyl and the other entries listed on the certificate of analysis. Results are reported per analyte in µg/g (ppm); totals (e.g. Total DDTs, Total Chlordanes) are calculated sums.
Pesticides

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